Supel^TM QuE分散SPE，柠檬酸提取管

NB.21

分散SPE法，通常也是指"QuEChERS” 方法(快速，简便，便宜，有效，耐用和安全)，是一种现代样本准备技术，正在越来越多地被用在食品和农业产品多残基杀虫剂分析领域。

使用QuEChERS方法，食品/农产品样本首先在水溶性溶剂(比如乙腈)，在高盐(比如氯化钠和硫酸镁)和或者缓冲试剂(比如柠檬酸盐)存在下，进行提取。高盐能够引起液相分离，而缓冲试剂能够稳定酸碱不稳定杀虫剂。 在摇晃和离心之后，有机相部分就进一步用SPE清洁。 和传统的SPE管方法不同，在分散SPE中，清洁需要混合大量的SPE(比如Supelclean PSA, ENVI-Carb， 和或者Discovery DSC-18)和提取物。 在样本清洁后，混合物经过离心，得到的上清可以直接分析，或者在分析前需要很少的处理。

Supelco有一系列的管和离心管，含有预置量的盐和SPE吸附剂，能够支持现今最常用的方法。

Supel^™ QuE Z-Sep products enhance sample cleanup for complex matrices by effectively removing more fat and color from sample extracts than traditional phases for QuEChERS methods. By eliminating problematic matrix interferences, Z-Sep products provide more robust LC-MS and GC-MS methods. This proprietary technology can replace C18 and PSA in your current methods without additional method development.

Z-Sep+ is recommended for cleanup of samples containing greater than 15% fat.
Z-Sep/C18 is recommended for cleanup of samples containing less than 15% fat.
Z-Sep is recommended for cleanup of samples prior to analysis of hydrophobic analytes.

Certain uses of this product may be covered by the claims of one or more pending patent applications. For licensing inquiries please contact techserv@sial.com
AOAC is a registered trademark of AOAC International
Discovery is a registered trademark of sigma-aldrich Co. LLC
Supel is a trademark of sigma-aldrich Co. LLC

polypropylene tube

100

Supel^™

Discovery^® DSC-18, 300 mg
Z-Sep, 120 mg

pk of 50

QuEChERS: suitable

15 mL , Shaker Compatible

zirconia-based phase

food and beverages

Compatible with most QuEChERS shakers.

11 - Combustible Solids

WGK 3